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排序方式: 共有610条查询结果,搜索用时 14 毫秒
1.
利用QuEChERS技术结合液相色谱-串联质谱联用法建立同时测定植物源性食品中6种双酰胺类农药残留的方法。样品采用乙腈作为提取剂,在缓冲盐环境下经振荡提取,C18、PSA和GCB净化,样液过膜后经C18柱分离,在电喷雾离子源、正离子扫描模式下多反应监测方式检测,基质配标,外标法定量。6种双酰胺类农药残留在0.1~150.0μg·L-1浓度范围内线性良好,相关系数大于0.995;加标回收率为64.3%~106.0%,相对标准偏差为1.6%~9.7%,检出限为0.1~1.0μg·kg-1。该方法简便、准确、灵敏,是同时测定植物源性食品中6种双酰胺类农药残留的有效方法。 相似文献
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随着空中交通的信息传输与新应用拓展需求不断增加,1090ES信号容量有限问题日益显现,对1090ES信号进行容量扩充是一种有效解决途径。针对一种基于脉内调相的1090ES信号扩容技术,给出了叠加调制的信号模型,研究了1090ES信号的解调解码算法;在GNU Radio+ USRP软件无线电平台上,实现了1090ES扩容信号的产生和接收处理,包括脉冲位置调制(Pulse Position Modulation,PPM)与8PSK叠加调制、低通滤波、报头检测、载波同步、PPM解码和相位解调等,并利用Matlab对实验的解码错误率和信号的频谱特性做了统计分析与仿真,结果表明了该扩容技术的可行性。 相似文献
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针对多源信号关联难度大、关联准确率低的问题,利用同一目标平台上搭载的多个辐射源信号具有一致的动态变化趋势这一特点,提出一种利用相位差特征的多源信号关联方法。已知阵列形式和侦测点位置,通过对侦收到的多个辐射源信号进行处理,获取相位差信息并累积形成相位差变化趋势;对比提取疑似相似段,根据相似性判决策略进行有效关联。该方法能有效避免不同传感器对位置测量的误差影响,相比传统基于位置信息关联的方法,能有效提升关联准确率。仿真和实测数据分析证明了该方法的有效性,在阵列形式和侦测点位置已知的条件下该方法具有重要工程意义。 相似文献
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Khaldoon Al-Htaybat Zaidoon Alhatabat 《Accounting Education: An International Journal》2018,27(4):333-357
The global digital revolution has irrevocably transformed societies and industries. The accounting profession is predicted to experience a significant change in the future, due to technological developments. Practices will be automated and related positions obsolete, thus accounting graduates need to be educated for new and different tasks and positions. The current study focussed on these expected changes and how accounting profession, practice and, consequently, education will be affected and adjusted to these new technologies in an evaluation approach. A qualitative methodology was employed, investigating accounting educators’ perceptions of these developments. Semi-structured interview data and online accessible empirical data, such as podcasts, were analysed in two coding cycles. The findings illustrate that while significant changes are expected, participants’ opinions vary regarding the necessity of adjusting the accounting curriculum. Supportive changes include amending respective courses to emphasise classic skills, such as problem-solving, and contemporary skills, such as new technologies, to illustrate developments practically. 相似文献
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Michael Atkins Sasikiran Nunna Komal Gupte-Singh Michael Eaddy 《Journal of medical economics》2018,21(2):212-217
Aims: The utilization of healthcare services and costs among patients with cancer is often estimated by the phase of care: initial, interim, or terminal. Although their durations are often set arbitrarily, we sought to establish data-driven phases of care using joinpoint regression in an advanced melanoma population as a case example.Methods: A retrospective claims database study was conducted to assess the costs of advanced melanoma from distant metastasis diagnosis to death during January 2010–September 2014. Joinpoint regression analysis was applied to identify the best-fitting points, where statistically significant changes in the trend of average monthly costs occurred. To identify the initial phase, average monthly costs were modeled from metastasis diagnosis to death; and were modeled backward from death to metastasis diagnosis for the terminal phase. Points of monthly cost trend inflection denoted ending and starting points. The months between represented the interim phase.Results: A total of 1,671 patients with advanced melanoma who died met the eligibility criteria. Initial phase was identified as the 5-month period starting with diagnosis of metastasis, after which there was a sharp, significant decline in monthly cost trend (monthly percent change [MPC]?=?–13.0%; 95% CI?=?–16.9% to –8.8%). Terminal phase was defined as the 5-month period before death (MPC?=?–14.0%; 95% CI?=?–17.6% to –10.2%).Limitations: The claims-based algorithm may under-estimate patients due to misclassifications, and may over-estimate terminal phase costs because hospital and emergency visits were used as a death proxy. Also, recently approved therapies were not included, which may under-estimate advanced melanoma costs.Conclusions: In this advanced melanoma population, optimal duration of the initial and terminal phases of care was 5 months immediately after diagnosis of metastasis and before death, respectively. Joinpoint regression can be used to provide data-supported phase of cancer care durations, but should be combined with clinical judgement. 相似文献
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张飞 《中国口岸科学技术》2021,(3):72-78
三七中药材产品经乙腈提取,盐析,采用C18和硅胶固相萃取柱净化后,用气相色谱仪检测38种有机氯、拟除虫菊酯农药残留含量。结果表明:C18和硅胶固相萃取柱净化能够有效除去三七药材中挥发油、有机酸、皂苷等大部分共萃物和干扰组分,获得较好的净化效果;3个不同浓度水平添加回收率在78.6%~120.3%之间,相对标准偏差为0.1%~12.5%;校准曲线线性相关系数均大于0.999。该方法操作简单、快速稳定、除杂效果明显,适用于三七中药材产品中多种农药残留的日常检测工作。 相似文献