| N-氯代邻苯二甲酰亚胺的合成研究 |
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| 引用本文： | 魏清,李建生.N-氯代邻苯二甲酰亚胺的合成研究[J].化工科技市场,2008,31(8). |
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| 作者姓名： | 魏清 李建生 |
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| 作者单位： | 1. 天津化工研究设计院,天津,300131
2. 天津职业大学 |
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| 摘 要： | 以苯酐为原料,与尿素反应制得邻苯二甲酰亚胺后,采用在醋酸水溶液中滴加次氯酸钠的方法制备N-氯代邻苯二甲酰亚胺,优化了反应的各种条件,使产品收率达94%以上.
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| 关 键 词： | N-氯代邻苯二甲酰亚胺 苯酐 邻苯二甲酰亚胺 氯代 |
Study on synthesis of N-chlorophthalimide |
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| Wei Qing,Li Jiansheng.Study on synthesis of N-chlorophthalimide[J].Chemical Technology Market,2008,31(8). |
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| Authors: | Wei Qing Li Jiansheng |
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| Institution: | Wei Qing~1 Li Jiansheng~2Tianjin Research , Design Institute of Chemical Industry,CNOOC,Tianjin 300131,China,Tianjin Professional College |
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| Abstract: | Phthalimide was synthesized by the reaction between phthalicanhydride and area.Then N-chlorophthalim- ide was prepared by droping hypochlorite into the solution of acetic acid,water and phthalimide.The reaction condition was optimized,and the product yield reached to over 94%. |
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| Keywords: | N-chlorophthalimide phthalimide acetic acid sodium hypocholrite chlorization |
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