| 四组分一锅法合成三苯胺-吡啶衍生物 |
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| 引用本文： | 张 欣,刘 霞,冯国良,张红利,耿丽君.四组分一锅法合成三苯胺-吡啶衍生物[J].河北工业科技,2011,28(3):142-,152. |
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| 作者姓名： | 张 欣 刘 霞 冯国良 张红利 耿丽君 |
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| 作者单位： | 河北科技大学理学院,河北石家庄,050018 |
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| 摘 要： | 以三苯胺醛、苯乙酮、3-氰基乙酰基吲哚和醋酸铵为原料,分别在传统加热回流和微波辐射条件下,利用四组分一锅法反应,简便地合成了一系列的三苯胺一吡啶衍生物.该方法具有产率较高、操作简单等优点.产物的结构通过了1H NMR,IR和E.A.表征.
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| 关 键 词： | 多组分反应 吡啶衍生物 三苯胺醛 3-氰基乙酰基吲哚 微波辐射 |
| 收稿时间： | 2010/11/3 0:00:00 |
| 修稿时间： | 2011/3/15 0:00:00 |
Four-component one-pot synthesis of triphenylamine-pyridine derivatives |
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| ZHANG Xin,LIU Xi,FENG Guo-liang,ZHANG Hong-li and GENG Li-jun.Four-component one-pot synthesis of triphenylamine-pyridine derivatives[J].Hebei Journal of Industrial Science & Technology,2011,28(3):142-,152. |
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| Authors: | ZHANG Xin LIU Xi FENG Guo-liang ZHANG Hong-li and GENG Li-jun |
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| Institution: | (College of Sciences,Hebei University of Science and Technology,Shijiazhuang Hebei 050018,China) |
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| Abstract: | A series of triphenylamine-pyridine derivatives were synthesized by four-component one-pot reaction of triphenylamine aldehyde,acetophenone,3-cyanoacetyl indole and ammonium acetate at refluxing temperature and microwave irradiation.This method has the advantages of good yield and easy operation.The structures of the products were characterized by 1H NMR spectra,IR and elemental analysis. |
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| Keywords: | multicomponent reaction pyridine derivatives triphenylamine aldehyde 3-cyanoacetyl indole microwave irradiation |
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