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| 纳米氧化锡粉体的制备及性能表征 | |
| 引用本文： | 魏妙丹,庞雪蕾,王 磊,李旭峰.纳米氧化锡粉体的制备及性能表征[J].河北工业科技,2011,28(6):351-354,358. |
| 作者姓名： | 魏妙丹 庞雪蕾 王 磊 李旭峰 |
| 作者单位： | 1. 河北华旭药业有限责任公司,河北石家庄,050031 2. 河北科技大学理学院,河北石家庄,050018 3. 石家庄铁道大学材料科学与工程学院,河北石家庄,050043 4. 河北工业职业技术学院,河北石家庄,050000 |
| 摘 要： | 以SnCl4·5H2O为主要原料,以十六烷基铵为分散剂,NH3·H2O作为沉淀剂,利用液相沉积法成功制备出了SnO2纳米颗粒.通过透射电镜(TEM)、X射线衍射(XRD)以及热重分析(TG),研究了纳米氧化锡粉体的形貌、尺寸分布和结构特征.SnO2颗粒平均粒径在30 nm左右,呈不规则多面体,有些近似于球形,粒径分布窄... |
| 关 键 词： | 液相沉积法 氧化锡(SnO2) 纳米SnO2 |
| 收稿时间： | 2011/6/22 0:00:00 |
| 修稿时间： | 2011/9/20 0:00:00 |
Preparation and characterization of nano-tin oxide powder |
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| WEI Miao-dan,PANG Xue-lei,WANG Lei and LI Xu-feng.Preparation and characterization of nano-tin oxide powder[J].Hebei Journal of Industrial Science & Technology,2011,28(6):351-354,358. | |
| Authors: | WEI Miao-dan PANG Xue-lei WANG Lei and LI Xu-feng |
| Institution: | WEI Miao-dan1,PANG Xue-lei2,WANG Lei3,LI Xu-feng4 (1.Hebei Huaxu Pharmaceutical Company Limited,Shijiazhuang Hebei 050031,China,2.College of Sciences,Hebei University of Science and Technology,Shijiazhuang Hebei 050018,3.College of Material Science and Engineering,Shijiazhuang Tiedao University,Shijiazhuang Hebei 050043,4.Hebei Institute of Vocation and Technology,Shijiazhuang Hebei 050000,China) |
| Abstract: | By using hexadecylamine as surfactant and stannic chloride pentahydrate as precursor,SnO2 nanoparticles are prepared by chemical precipitation method in ammonia solution.The crystal pattern,size distribution and morphology of the nanoparticles are studied with TEM,XRD and TG.The size of the particles is about 30 nm.The particles present irregular polyhedron or near-spherical morphology.The nano-particles have narrow size distribution and good dispersibility.The size of the nano-tin oxide powder could be inf... |
| Keywords: | liquid phase deposition tin oxide(SnO2) nano SnO2 |
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