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主要研究了以N-甲基二乙醇胺(MDEA)在CuO/Cr2O3/Al2O3催化剂催化下脱氢制备4-甲基-2-吗啉酮(MMO),采用FT-IR、1H-NMR、GC-MS对MMO进行了表征,实验成功制备了MMO;考察催化剂的组分和比例对脱氢制备MMO的影响,结果表明当催化剂nCu:nCr:nAl=2:2:1时,CuO/Cr2O3/Al2O3催化剂的脱氢效果最为理想;研究反应条件对MMO的产率、转化率,确认最佳反应条件是反应温度为260°C-320°C,氢醇比为5.2-6.2,MDEA转化率达到100%,同时MMO产率最高达99.8%。 相似文献
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简单的分析了铜基复合材料的优良特性,简要的综述了制备铜基复合材料的方法;在粉末冶金工艺的基础上,利用自己设计的电阻快速烧结系统,成功地制备了Al3O2/Cu复合材料,并且利用光学显微镜对所烧结的复合材料试样进行了对比观察分析,证明了系统的可行性及实用性。 相似文献
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简单的分析了铜基复合材料的优良特性,简要的综述了制备铜基复合材料的方法;在粉末冶金工艺的基础上,利用自己设计的电阻快速烧结系统,成功地制备了Al3O2/Cu复合材料,并且利用光学显微镜对所烧结的复合材料试样进行了对比观察分析,证明了系统的可行性及实用性。 相似文献
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采用气相色谱法,测定了不同加工工艺对速冻毛豆中的毒死蜱残留量的影响。结果表明,各种加工工艺对速冻毛豆中的毒死蜱残留都有不同程度的去除作用。热烫时间越长,毒死蜱残留量越低,98℃热烫180s后,残留下降43.7%;相同时间内,清水浸泡洗涤的去除率为47.0%,15%盐水浸泡洗涤的去除率为81.1%;固定浓度O3处理时间越长,毒死蜱残留量越低,相同时间内,浓度越高的O3处理,毒死蜱的去除率越高,经5mg/kgO3处理30min,去除率为40.3%;H2O2处理也具有与O3处理相同的作用,经3.0mL/LH2O2作用30min,去除率为57.3%。结果显示,适当延长加工工艺中的热烫时间,或采用盐水浸泡的生产工艺,或是采用O3或H2O2处理的生产工艺,均能有效降低速冻毛豆中毒死蜱的残留量。 相似文献
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闪光烧结的辐照面积大,能量密度分布均匀,可以显著提高天线3D打印的生产效率。目前对闪光烧结工艺的研究较少,烧结机理及其影响因素认识不足。为解决上述问题,针对纳米银薄膜闪光烧结工艺过程建立了数值模型,研究了纳米银薄膜和基板的温度分布规律,揭示了辐照能量对烧结温度的影响规律。实验测量了烧结温度和电导率,电导率最高为3.09×107 S/m,验证了模型的准确性。利用喷墨打印和闪光烧结制备了微带天线,实测其中心频率为5.81 GHz,在中心频率处回波损耗为-24.5 dB,与设计值吻合较好。仿真和实验成果可以为闪光烧结工艺的应用提供理论指导。 相似文献
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本文阐述了近十年来加氢脱硫催化剂的一些进展,其中包括催化剂主要成分活性组分、载体的一些变化,并阐述了改进后的催化剂产生的新性能。其中,对于催化剂的加氢脱硫活性为Co-Mo<Ni-Mo>Ni-W,对不同的工业过程可采用不同的催化剂组合,载体除了传统的y-Al2O3外,近年来还研究了TiO2,ZrO2,复合氧化物,介孔分子筛或沸石等载体,具有较高的活性。在制备方式上,传统的加氢脱硫催化剂主要采用浸渍法,将金属组分直接浸渍于y-Al2O3载体上,然后进行干燥、焙烧即得氧化态的催化剂。近年来,也出现了采用免焙烧式的加工工艺,以FCC汽油重馏分为原料,实验得免焙烧式的催化剂有很高的加氢脱硫活性。 相似文献
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研究了固体超强酸SO42-/TiO2-SnO2-Al2O3催化衣康酸与异辛醇合成衣康酸二异辛酯的酯化反应,甲苯作为带水剂,考察了催化剂种类,确定以SO24-/TiO2-SnO2-Al2O3为催化剂。随后考察反应物配比、催化剂用量、反应时间等因素对酯化反应的影响,确定了最佳工艺条件为n(衣康酸):n(异辛醇)=1:3,催化剂用量4.5%(质量分数),反应时间2h。在该条件下,衣康酸转化率达到98.9%,产物衣康酸二异辛酯的收率为96.2%。并对SO24-/TiO2-SnO2-Al2O3的重复使用性能进行考察,结果表明,与SO24-/TiO2相比,SO42-/TiO2-SnO2-Al2O3在重复使用5次后仍具有较高的催化活性,衣康酸转化率和衣康酸二异辛酯收率为分别为98.2%和95.7%,说明载体中添加Sn和Al对于增加固体超强酸的寿命起了主要作用。 相似文献
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《化工科技市场》2002,(12)
一种氧化铁超细纳米粉体的制备方法公开号 CN 1364730A 公开日 2002.8.21申请人 无锡威孚吉大新材料应用开发有限公司摘要 本发明涉及氧化铁超细纳米粉体的制备方法,属于精细化工领域。本发明利用廉价的铁盐化工原料批量制备氧化铁(α-Fe2O3,γ-Fe2O3,Fe3O4)超细纳米粉体,粉体的晶粒尺寸接近单分散,其平均粒径分别为10~20nm(α-Fe2O3)、3~10 nm(γ-Fe2O3)和5~15 nm(Fe3O4)。本发明具有工艺简单、设备投入成本低、粉体超细以及产量高的优点,非常适合规模化生产。在催化剂、磁性材料、颜料和涂料、敏感器件、医用材料等诸多领域都有广阔的应用前景。 相似文献
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《中国对外贸易(英文版)》2008,(5):50-51
The overall strategic relationship between U.K. and China is "better than ever", China- Britain relations have maintained good momentum, with increased high-level exchanges and the reinforcement of strategic mutual trust, with more room for growth in the future. 相似文献
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Guo Yan 《中国对外贸易(英文版)》2008,(5)
Domino effects of the global finance agitation As the origin of the subprime crisis,US financial institutions lost USS45 billion last year,accounted for over half of the total US,EU & Japan loss.Since January 15th,Chtigroup released its financial statement of the 4th quarter,showing a net deficit of USS9.83 billion,which marked the hisoric high of its quarterly deficit. 相似文献
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《中国对外贸易(英文版)》2008,(6):62-65
Among the Fortune 500 firms,more and more images from China emerge out.On the 2008 list,Sinosteel Corporation,a landmark group of China industries quietly squeezes into the candidate line.As the largest steel service & trade enterprise,its sales reached at RMB 111.24 billion,with a year-on-year increase of 83.03 percent,and the profit grew by 180.03 percent.On the Sinosteel 2008 Work Meeting,the president Huang Tianwen uttered,"In the coming year,we will work for US$20 billion sales,and look forward to getting a position in Fortune 500 firms for ourselves." 相似文献
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Zang Kejia 《中国对外贸易(英文版)》2008,(7):16-17
When the 103rd Canton Fair is approaching, an old friend of Canton Fair, Li Ying from Jiangsu prov-ince recollected his past five years' experiences to the grand trade meeting. Each year is special, with some unforgettable memories colored by the year. 相似文献
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Estaing, former French president, Valery Giscard d'Estaing attended Sino-French Economic Seminar held in Shanghai in early April and said that the world center has shifted from the west to the east with many European and US companies entering into Asia, and China has the ability to play an important role in the world stage. Estaing, naming himself"French Confucian", then said in Chinese that a cook-group includes 10 people in ancient Chinese soldier system and the cook is in charge of cooking for them. And people who belong to the same cook are actually "Partners". 相似文献
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《中国对外贸易(英文版)》2008,(5):12
The annual meeting of the World Economy Forum was held in Davos,a little town in Switzerland,on January 23rd to the 27th this year,with the theme"the Power fo Collaborative Innovation",over 2500 celebrates from ture political and cconomic circles of more than 80 countries and challengred logether to talk about the future of the global economy in 2008,A Forum for the problems and challenges that face whole world,some of the keywords which drew attention during the event were:the U.S.subprime mortgage crisis,soaring energy prices,the economic slowdown in the U.S.ermerging economic bodies,authority funds and the general unpredictable nature of the global economy. 相似文献
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"If you are considering to trade with companies in Japan or expanding your business to Japan we are ready to help from the very beginning."You will find this greeting at the first sight on the Chinese website of Japan External Trade Organization 《中国对外贸易(英文版)》2008,(10):16-17
If you are considering to trade with companies in Japan or expanding your .business to Japan, we are ready to help from the very beginning." You will find this greeting at the first sight on the Chinese website of Japan External Trade Organization (JETRO). JETRO has committed itself in delivering highly efficient and quality services to meet the demand of internal and external customs including Japanese companies, hence winning a good reputation in the international trade arena. In recent years, with its priority in advancing business cooperation in South and East Asia, JETRO has made great achievement in promoting trade between China and Japan. Therefore, China's Foreign Trade interviewed Mr. Yoichi Maine, Deputy Director General of JETRO BEIJING. 相似文献
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Guo Yan 《中国对外贸易(英文版)》2008,(12):62-63
Looking at the increasingly fierce competition in the world auto market. global automobile manufacturing industry, taking Europe, the U.S. and Japan as representatives, is gradually forming a new type of relationship, mutual cooperation between whole vehicle and parts manufacturers. We can clearly see that auto parts manufacturers have become independent from the whole vehicle manufacturing companies, which means that the former structure of auto industry has greatly changed, and a new relationship, 相似文献
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Guo Yan 《中国对外贸易(英文版)》2008,(1):10-10
In the middle of last December, the key purchase contracts for coal used in power generation in 2008 were signed, reflecting a demand for more than 1.085 billion tons. It is important to note that the country's five biggest power producers, China Huaneng Group, China Guodian Corporation, China Power Investment Corporation, China Huadian Corporation and China Datang Corporation, had settled on the prices on their purchase contracts, and they are expected to consume 290 million tons of coal for generating electricity, 相似文献
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Liu Xinwen 《中国对外贸易(英文版)》2008,(10):40-41
Last November the State Council of China decided to renew its holiday system by reducing the seven-day May Day holiday to three days and introducing three new one-day public holidays, namely the Qingming Festival, Dragon Boat Festival and Moon Festival. By doing so, the three golden-week holidays that were introduced in 1999, namely the Spring Festival, May Day and National Day, could be better distributed. 相似文献