| 静态顶空气相色谱法测定地表水中苯系物 |
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| 引用本文： | 苟德国,黄忠平,陈京京,张晓勇.静态顶空气相色谱法测定地表水中苯系物[J].中国资源综合利用,2011,29(3):41-43. |
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| 作者姓名： | 苟德国 黄忠平 陈京京 张晓勇 |
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| 作者单位： | 1. 大丰市环境监测站,江苏,大丰,224100
2. 江苏省环境监测中心,南京,210036 |
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| 摘 要： | 采用静态顶空气相色谱—氢火焰离子化检测器法（HS-GC-FID）测定地表水中8种苯系物,对其分析条件进行了优化,详细讨论了分析过程中各因素对测定结果的影响。结果发现,CP-WAX52CB极性石英毛细管柱可以实现水中苯系物的各组分完全分离,苯系物各组分线性方程的相关系数均大于0.990,方法检出限为1.6~3.5μg/L,加标回收率为93.3%~101.4%之间,相对标准偏差为2.28%~3.82%（n=6）。该方法准确、快捷、线性范围广,适用于饮用水和地表水中低浓度挥发性苯系物的测定。
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| 关 键 词： | 静态顶空气相色谱法 苯系物 地表水 |
Detection of BTEX in Water by Static Headspace-gas Chromatography |
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| Gou Deguo,Huang Zhongping,Chen Jingjing,Zhang Xiaoyong.Detection of BTEX in Water by Static Headspace-gas Chromatography[J].China Resources Comprehensive Utilization,2011,29(3):41-43. |
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| Authors: | Gou Deguo Huang Zhongping Chen Jingjing Zhang Xiaoyong |
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| Institution: | Gou Deguo1,Huang Zhongping1,Chen Jingjing1,Zhang Xiaoyong2(1.Dafeng Environmental Monitoring Station,Dafeng 224100,China,2.Jiangsu Environmental Monitoring Center,Nanjing 210036,China) |
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| Abstract: | A method for the determination of BTEX in surface water with static headspace gas chromatography and flame ionization detector(HS-GC-FID) was developed in the paper.To characterize the performance of this method,several parameters were studied in some detail,such as the polarity of capillary column,the volume ratio of the gas phase and the liquid phase,equilibration temperature and equilibration time.It was found that the components could be separated with the CP-WAX52CB capillary column completely.The coef... |
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| Keywords: | static headspace gas chromatography BTEX surface water |
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