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采用LC-ICPMS测定EN71-3玩具中的可迁移铬(三价铬&六价铬)方法,通过确认,本方法完全满足标准中第三类玩具样品的测试要求。 相似文献
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选择国内企业生产的不锈钢供水管道,用余氯和硬度分别为2、100 mg/L的浸泡液浸泡24 h,并检测水质中六价铬的变化。结果显示,浸泡液中的六价铬变化与不锈钢供水管道的工艺有很大关系,焊缝处理、打磨抛光、酸洗钝化三个条件都对六价铬的迁移有很大影响。 相似文献
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本文研究了软泥类玩具材料中硼酸和硼酸盐含量的检测方法,用0.07 mol/L盐酸溶液提取试样,电感耦合等离子体质谱KED模式分析同位素11B,通过硼元素的含量换算成硼酸和硼酸盐来确定软泥类玩具材料中硼酸和硼酸盐的含量。硼元素浓度在2~1000μg/L与其响应值呈线性关系(R^2=0.99984),硼元素、硼酸、硼酸盐的检出限分别为0.042 mg/kg、0.240mg/kg和0.369 mg/kg,定量限分别为0.100 mg/kg、0.572 mg/kg和0.883 mg/kg,加标回收率为87.5%~105.3%,相对标准偏差(RSD,n=7)小于5%。该方法准确度高、精密度好,满足软泥类玩具材料中硼酸和硼酸盐的测定。 相似文献
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本文参照EN71-3黏稠性玩具样品处理方法,建立了电感耦合等离子体质谱法(ICP-MS)测定水晶泥玩具材料中硼元素迁移量的检测方法。对该方法的同位素选择、线性范围和检出限、加标回收率和精密度、实际样品测试等进行了讨论。结果表明,该方法的线性范围宽,ICP-MS测定硼元素线性相关系数可达0.9996,该方法加标回收率为90.60%,相对标准偏差在4.40%。建立的ICP-MS法测定水晶泥玩具材料中硼元素具有检出限低、精密度高、简便快速等优点,可用于水晶泥玩具材料中硼元素迁移的定量分析。 相似文献
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HPLC法快速测定果汁饮料中胭脂虫红的含量 总被引:1,自引:0,他引:1
建立了不同类型的饮料中胭脂虫红含量测定的高效液相色谱法。HPLC色谱条件:以C_(18)作为分离柱;流动相为乙腈-0.5%H_3PO_4溶液(80:20);流速1.0 mL/min;检测波长275 nm;进样量10μL。本方法胭脂虫红检出限为0.1 mg/kg,回收率为88.9%~98.6%,相对标准偏差为1.87%~3.14%。 相似文献
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本文阐述了玩具中特定元素迁移的危害、标准限量及国内外安全监管现状.讨论了特定元素迁移的测试方法及结果分析,并对控制玩具材料特定元素迁移提出了对策建议。 相似文献
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建立检测牛血液样品中莱克多巴胺、克伦特罗、沙丁胺醇和马布特罗等4种β-兴奋剂类药物的高效液相色谱质谱联用方法(LC-MS/MS)。采用β-葡萄糖醛酸苷酶对牛血液样品进行水解,采用pH 5.2的乙酸钠溶液对样品进行提取,通过固相萃取柱净化样品,浓缩提取物。在正离子模式下,采用多反应监测(MRM)模式对β-受体激动剂进行定性和定量分析,通过三个浓度水平(0.5μg/L、1.5μg/L、4.0μg/L)进行验证试验。所得样品回收率在95.4%~101.9%之间,相对标准偏差(RSD)在0.84%~8.56%。该方法具有简便、准确的优点,各项技术指标均符合国内外法规的要求,能够确证检测牛血液中β-受体激动剂类药物残留。 相似文献
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Chun Yi 《中国对外贸易(英文版)》2008,(6)
In recent years.China's public finance put social construction high on the agenda and attaches more importance on livelihood insurance and improvement.The 2003-2007 public financial expenditure reflects a fact that the government isputting more emphasis on livelihood andissues concerning the people. 相似文献
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《中国对外贸易(英文版)》2008,(6)
"Crucial for economic growth.energy utilization has its role in all economic sectors and every aspect of people's daily life.Now we are in dire need of a new profession,namely energy manager.We not only need to have passion and responsibility,but also a scientific approach to conserve energy and cut emissions.APpropriate legislation should be in place.and a special profession should be introduced to ensure the implementation of these laws and regulations." 相似文献
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According to Ma Kai's economic planning report submitted to the NPC session on March th. 《中国对外贸易(英文版)》2008,(6):15-15
According to Ma Kai's economic planning report submitted to the NPC session on March 5th,(Ma Kai is the Minister in charge of the National Development and Reform Commission),the government has listed the slowdown in trade surplus growth and the steady expansion of external investment as major tasks for 2008. 相似文献
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《中国对外贸易(英文版)》2008,(1):64-67
A bout fifty years ago. a baby's cry broke the sky of quietness, in a small and beautiful town of Hunan province, which surroundcd by green hills and clear water. Though his .birth brought his family great happiness and hope just as any new life, nobody knew that the little boy would get great achievement when he grow up. even start his business oversea, and earn international honor. Let's share with you the entrepreneur Ouyang Riping's story, which may insights thcsc people who want to succeed and complete oneself in favorite condition or adversity rather leave things to so-called fate. 相似文献
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Liu Xinwen 《中国对外贸易(英文版)》2008,(5):44-45
"In recent years, we've found increasing interest from Chinese investors in the Belarus economy. Please let China know, Belarus is always ready to be a true friend to China. We have built a fort in Europe for China," the President of Belarus, Alexander Lukashenko told Zhou Xiaochuan, President of the Bank of China, during his visit to the capital of Minsk, on January 8th, he expressed his high praise and firm confidence in the development of Sino-Belarusian relations. 相似文献
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《中国对外贸易(英文版)》2008,(5):34-35
Similar to what the Christmas Day means for the westerners,the Spring Festival is the most important celebration for Chinese people.This big event according to Chinese traditional lunar calendar relaxes and pleases the whole country as the happiest gathering time of the year.National-wide crusade for going back home,too-difficult-to-get train tickets,generous family-going-out shopping,Miaohui laundering,New Year Eve reunion dinner,visiting friends and relatives,watching annual TV gala......each piece of clue reminds us of the smell of Chinese Spring Festival. 相似文献
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《中国对外贸易(英文版)》2008,(5):21
FDI(Foreign Direct Investment),a component of a country's national financlal accounts,is investment of foreign assets into domestic structures,equipment,and organizations.It does not include foreign investment into the stock markets,concession and subcontract.FDI iS thought to be more useful to a country than investments in the equity of its companies because equity investments are potentially "hot money"which can leave at the first sign of trouble,whereas FDI is durable and generally useful whether things go well or badly. 相似文献
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Holding percent of train media resources across China based on "Time Cube" on the Intermedia Recommendation Introduction Meeting on December HTC announced its high-profile strategy of tour marketing tapping the immeasurable potentials on the train. Meanwhile HTC officially launched its brand new product Olympic Train on the meeting providing a fabulous platform for all the brands that are prepared to do a smart marketing on the occasion of Olympic Games.…… 《中国对外贸易(英文版)》2008,(1):58
Holding 88 percent of train media resources across China, based on "Time Cube", on the 2008 Intermedia Recommendation and Introduction Meeting on December 19, 2007, HTC announced its high-profile strategy of tour marketing and tapping the immeasurable potentials on the train. Meanwhile, HTC officially launched its brand new product Olympic Train on the meeting, providing a fabulous platform for all the brands that are prepared to do a smart marketing on the occasion of 2008 Olympic Games. 相似文献
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Audrey Guo 《中国对外贸易(英文版)》2008,(1)
In the end of 2007, Air China Limited (hereinafter "Air China") and Shanghai Airlines, formally joined Star Alliance at a ceremony held in the new Terminal Three at Beijing Capital International Airport. With the addition of the two Chinese airlines, Star Alliance now has 19 member carriers operating 17,000 daily flights to 897 destinations in 160 countries. 相似文献
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《中国对外贸易(英文版)》2008,(5):50-51
The overall strategic relationship between U.K. and China is "better than ever", China- Britain relations have maintained good momentum, with increased high-level exchanges and the reinforcement of strategic mutual trust, with more room for growth in the future. 相似文献