| 三氯异氰尿酸红外光谱测绘方法探讨 |
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| 引用本文： | 刘红梅,何书美,王晓凤,葛艳蕊.三氯异氰尿酸红外光谱测绘方法探讨[J].河北工业科技,2000,17(4):18-20. |
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| 作者姓名： | 刘红梅 何书美 王晓凤 葛艳蕊 |
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| 作者单位： | 1. 河北科技大学化学与制药工程学院,河北石家庄,050018
2. 河北师范大学实验中心,河北石家庄,050016 |
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| 摘 要： | 对 KBr压片法、KCl压片法及萨特勒图谱采用的糊状法所绘制的三氯异氰尿酸的红外光谱图进行了分析、对照。同时将三氯异氰尿酸分别与 KBr,KCl研磨 ,以及三氯异氰尿酸纯品进行了可见 -紫外吸收光谱对照。实验发现 ,KCl压片法克服了溶剂的影响 ,更简单、直观体现了物质的精细结构 ,且与 KCl研磨后的三氯异氰尿酸的纯品图谱一致 ,说明结构未发生变化。因此认为 KCl压片法是绘制三氯异氰尿酸红外光谱图较好的方法
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| 关 键 词： | 三氯异氰尿酸 红外光谱 压片法 |
| 修稿时间： | 1999-12-03 |
Study on Determination Method of Trichloro-s-trlazine 2,4,6(1H,3H,5H)-trion by I.R.Spectrometry |
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| LIU Hong-mei,HE Shu-mei,WANG Xiao-feng,GE Yan-rui.Study on Determination Method of Trichloro-s-trlazine 2,4,6(1H,3H,5H)-trion by I.R.Spectrometry[J].Hebei Journal of Industrial Science & Technology,2000,17(4):18-20. |
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| Authors: | LIU Hong-mei HE Shu-mei WANG Xiao-feng GE Yan-rui |
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| Abstract: | The paper makes a comparison among I.R.absorption spectrums of Thrichloro-s-trlazine-2,4,6(1H,3H,5H) trion which were gotten by KBr wafter,KC1 wafter and mu 11 technique used in Sadteler Infrared Spectroscopy Atlats.It has been found that KC1 wafter eliminated the effect of solvent and directly demonstrated the fine structure of material.The UV VIS absorption spectrum of Trichloro trlazine 2,4,6(1H,3H,5H) trion grinded in KCl is as the same as the pure sample,which indicates material structure has not changed.Therefore KC1 wafter is a satisfactory method to draw the I.R.spectrum of Trichloro s trlazine-2,4,6(1H,3H,5H)-trion. |
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| Keywords: | Trichloro s trlazine-2 4 6(1H 3H 5H) trion I R spectrum wafte? |
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